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Direct electrodeposition of hydrogenated reduced graphene oxide from unsonicated solution and its electrochemical response

dc.contributor.authorNoce, R.D.
dc.contributor.authorEugenio, S.
dc.contributor.authorSiwek, K. I.
dc.contributor.authorMoura E Silva, Teresa
dc.contributor.authorCarmezim, Maria
dc.contributor.authorSakita, A. M. P.
dc.contributor.authorLavall, R.L.
dc.contributor.authorMontemor, M.F.
dc.date.accessioned2020-05-06T15:16:24Z
dc.date.available2020-05-06T15:16:24Z
dc.date.issued2020-04
dc.description.abstractReduced graphene oxide (rGO) is successfully electrodeposited from a graphene oxide-containing suspension under stirring and no sonication onto Ni foam by applying -1.5 V/SCE. The electrodeposited material is characterized by X-Ray Diffraction (XRD), Scanning electron microscopy (SEM), Raman spectroscopy, Fourier Transform Infra-Red spectroscopy (FTIR) and Thermogravimetric analysis (TGA). FTIR and TGA results indicate the formation of hydrogenated rGO after electrodeposition. In addition, the electrochemical response of the rGO/Ni electrode is evaluated by cyclic voltammetry in 1 M potassium hydroxide solution. The results reveal that the electrode possesses higher conductivity and lower polarization loss compared to bare Ni foam, opening wider perspectives to design composites with improved electrochemical performance.pt_PT
dc.description.versioninfo:eu-repo/semantics/publishedVersionpt_PT
dc.identifier.citationDELLA NOCE, R.; [et al] – Direct electrodeposition of hydrogenated reduced graphene oxide from unsonicated solution and its electrochemical response. Diamond and Related Materials. ISSN 0925-9635. Vol. 104 (2020), pp. 1-6pt_PT
dc.identifier.doi10.1016/j.diamond.2020.107740pt_PT
dc.identifier.issn0925-9635
dc.identifier.urihttp://hdl.handle.net/10400.21/11598
dc.language.isoengpt_PT
dc.peerreviewedyespt_PT
dc.publisherElsevierpt_PT
dc.relationM-ERA.NET/0004/2014 - FCTpt_PT
dc.relation.publisherversionhttps://pdf.sciencedirectassets.com/271601/1-s2.0-S0925963520X00033/1-s2.0-S0925963519308118/main.pdf?X-Amz-Date=20200506T150119Z&X-Amz-Algorithm=AWS4-HMAC-SHA256&X-Amz-Signature=b33bcffdef4c388fc870401e35596e3ed0cded9b185d574e669bcef56f8ac88e&X-Amz-Credential=ASIAQ3PHCVTY366J365A%2F20200506%2Fus-east-1%2Fs3%2Faws4_request&type=client&tid=prr-3c2f73a0-ef36-44a1-bc11-b8927e01f54b&sid=b26d6a1f6e496046332a35a6a047949fe8d9gxrqb&pii=S0925963519308118&X-Amz-SignedHeaders=host&X-Amz-Security-Token=IQoJb3JpZ2luX2VjEG8aCXVzLWVhc3QtMSJIMEYCIQCOojmOjFmdbp%2BbyAQEyyGaLsM%2FQGrhi2mAIFr7zw1qDwIhANysBWQKrktc8cQm7iO2cdxXddleZavhk0stMkSg5YDmKr0DCKf%2F%2F%2F%2F%2F%2F%2F%2F%2F%2FwEQAxoMMDU5MDAzNTQ2ODY1IgwoQGV%2FYEjThsh96R4qkQMevzaf39mzhQvFad%2BN4nTJP2QTCeUrysI3kctr8Qpo111i2tMHPcR%2BE6%2BqhRyWilvWzoYRUO8EiihGOh4jw1VDEIgHctQ7%2BjJqIV7YOAX%2BCdbyh4WWF%2FD3X2yXk%2FjQmLK3u2%2F%2FiHMrWybXwllkZaoMC5bTgXk%2F5cwimBuOINCS0IVtb8A6AEfYEhxSTGRLDDNeV2ldXFz2NSiFoIBXRvTGq0%2BZlu9G2bk2xUHeZTqs8TivSuRBhp0nZh3DyBrSjr4I6D0wZ4AMF7IVO2d5yo4aFdcd7y3PYm%2BP8ICFLcVU%2BWzWKYsJ5dvhx8T%2BDYdkowAeaGrzuUFbjH%2FiKAAINQu2eBW5MRXvqE4XFl%2Fbm98WoyBN8ughbNsJgZg5%2B5Tk0U93OzGU0GqMd1nBBslLz7C7V7qP0AhrMMaQq%2BlgyUmblEXSGQY%2BPGdZHSeeEjlgDVKSeGfPD4iW4mtSSUy92qvV433X%2BNQ0UxLuZMWFWA0PepjVN%2BXIXrwVReXFOGNBwsr830SGfemRRmxziZ31gTuDNzCaiMv1BTrqAfwGXL6n6kJxsc%2BM%2B3Mv4pI3y80rsvPXC9bSSpm9wC1CQpUuwtESfokIsGqT2%2Bw%2FCOsVLb1ABueJkuPVUluV5lchOFMiE13bw68x9V2jjHNJpd8XiVvhvxytVZ9HSwEV6%2FYJJO76yK4V1Bidf%2Fg5gVu%2BUZEReH3x6HGSjxyC6SgJXCMF4WFfMjMoCvOQBDXzNxtg0nBrCKX8DSJrK%2FxxOo%2BZJ5MIIUC3mhQaOpWtySmhzf1OGzhoraEW36CEnh39cWnDbE0ueEoH6GJcse3%2BsV6OzRfU5atJLPBGp7eAm1Y%2FQaOgcRWrhJr3%2Bg%3D%3D&host=68042c943591013ac2b2430a89b270f6af2c76d8dfd086a07176afe7c76c2c61&X-Amz-Expires=300&hash=8f319bc9b0f0fe0e52795e655cf9dfe185ba19071447f601770e52eb9a8cc3d0pt_PT
dc.subjectReduced graphene oxidept_PT
dc.subjectElectrodepositionpt_PT
dc.subjectCyclic voltammetrypt_PT
dc.titleDirect electrodeposition of hydrogenated reduced graphene oxide from unsonicated solution and its electrochemical responsept_PT
dc.typejournal article
dspace.entity.typePublication
oaire.awardURIinfo:eu-repo/grantAgreement/FCT/3599-PPCDT/M-ERA.NET%2F0002%2F2012/PT
oaire.awardURIinfo:eu-repo/grantAgreement/FCT/3599-PPCDT/PEst-OE%2FQUI%2FUI0100%2F2013/PT
oaire.citation.endPage6pt_PT
oaire.citation.startPage1pt_PT
oaire.citation.titleDiamond and Related Materialspt_PT
oaire.citation.volume104pt_PT
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oaire.fundingStream3599-PPCDT
person.familyNameDella Noce
person.familyNameMoura e Silva
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person.familyNamePerdizio Sakita
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person.givenNameTeresa
person.givenNameMaria
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project.funder.identifierhttp://doi.org/10.13039/501100001871
project.funder.identifierhttp://doi.org/10.13039/501100001871
project.funder.nameFundação para a Ciência e a Tecnologia
project.funder.nameFundação para a Ciência e a Tecnologia
rcaap.rightsclosedAccesspt_PT
rcaap.typearticlept_PT
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